Водородно-индуцируемые мартенситные превращения и двойникование в аустенитной нержавеющей стали AISI 321 при прокатке

Авторы

Elena G. Astafurova ¹ , Evgenii V. Melnikov ¹ , Sergey V. Astafurov ¹

¹ Лаборатория физики иерархических структур в металлах и сплавах, Институт физики прочности и материаловедения СО РАН, Академический пр., 2/4, Томск, 634055, Россия

10.17586/2687-0568-2024-6-3-120-131

Rev. Adv. Mater. Technol., 2024, vol. 6, no. 3, pp. 120–131

Аннотация

Исследовано влияние электролитического насыщения водородом (в растворе 1N H2SO4 с добавлением CS(NH2)2, при плотностях тока 10, 100 и 200 мА/см2 в течение 5 часов) на микроструктуру и фазовый состав аустенитной нержавеющей стали AISI 321 во время прокатки при комнатной температуре. Экспериментально показано, что насыщение стальных образцов водородом усиливает вклад механического двойникования в фрагментацию их структуры и способствует реализации γ→α' и γ→ε превращений во время прокатки. Как двойникование, так и мартенситные превращения зависят от режима наводороживания: увеличение плотности тока при насыщении образцов водородом вызывает уменьшение толщины двойниковых пластин, увеличивает плотность двойниковых границ и долю α'-мартенсита в структуре прокатанных образцов. Образование высокой плотности границ Σ3n (двойниковых и мартенситных) препятствует образованию разориентированной зеренной структуры в аустените при прокатке стальных образцов. Показано, что предварительное насыщение водородом обеспечивает более быструю кинетику фазового превращения γ→α' при прокатке метастабильной стали AISI 321.

Ключевые слова

аустенитная нержавеющая сталь; водород; двойникование; мартенситное превращение; микроструктура

Финансирование

Government research assignment for ISPMS SB RAS: FWRW-2022-0005

Ссылки

1.    K.H. Lo, C.H. Shek, J.K.L. Lai, Recent developments in stainless steels, Mater. Sci. Eng. R, 2009, vol. 65, no. 4-6, pp. 39-104.
2.    T. Michler, C. San Marchi, J. Naumann, S. Weber, M. Martin, Hydrogen environment embrittlement of stable austenitic steels, Int. J. Hydr. Energy, 2012, vol. 37, no. 21, pp. 16231-16246.
3.    R.A. Oriani, A mechanistic theory of hydrogen embrittlement of steels, Ber. Bunsengesellsch. Phys. Chem., 1972, vol. 76, no. 8, pp. 848-857.
4.    M. Nagumo, Fundamentals of hydrogen embrittlement, Springer, Singapore, 2016.
5.    S. Lynch, Hydrogen embrittlement phenomena and mechanisms, Corros. Rev., 2012, vol. 30, no. 3-4, pp. 105-123.
6.    H.K. Birnbaum, P. Sofronis, Hydrogen-enhanced localized plasticity-a mechanism for hydrogen-related fracture, Mater. Sci. Eng. A, 1994, vol. 176, no. 1-2, pp. 191-202.
7.    P.J. Ferreira, I.M. Robertson, H.K. Birnbaum, Hydrogen effects on the character of dislocations in high-purity aluminium, Acta Mater., 1999, vol. 47, no. 10, pp. 2991-2998.
8.    P. Rozenak, L. Levin, D. Eliezer, Hydrogen effects on phase transformations in austenitic stainless steels, J. Mater. Sci., 1984, vol. 19, no. 2, pp. 567-573.
9.    E.G. Astafurova, E.V. Melnikov, S.V. Astafurov, I.V. Ratochka, I.P. Mishin, G.G. Maier, V.A. Moskvina, G.N. Zakharov, A.I. Smirnov, V.A. Bataev, Hydrogen embrittlement effects on austenitic stainless steels with ultrafine-grained structure of different morphology, Phys. Mesomech., 2019, vol. 22, pp. 313-326.
10.    J. Morisawa, M. Kodama, S. Nishimura, K. Asano, K. Nakata, S. Shima, Effects of hydrogen on mechanical properties in irradiated austenitic stainless steels, J. Nuclear Mater., 1994, vol. 212-215, pp. 1396-1400.
11.    L.R. Queiroga, G.F. Marcolino, M. Santos, G. Rodrigues, C. Eduardo dos Santos, P. Brito, Influence of machining parameters on surface roughness and susceptibility to hydrogen embrittlement of austenitic stainless steels, Int. J. Hydr. Energy., 2019, vol. 44, no. 54, pp. 29027-29033.
12.    S. Weber, M. Martin, W. Theisen, Impact of heat treatment on the mechanical properties of AISI 304L austenitic stainless steel in high-pressure hydrogen gas, J. Mater. Sci., 2012, vol. 47, no. 16, pp. 6095-6107.
13.    D.P. Abraham, C.J. Altstetter, The effect of hydrogen on the yield and flow stress of an austenitic stainless steel, Metall. Mater. Trans. A, 1995, vol. 26, no. 11, pp. 2849-2858.
14.    D.P. Abraham, C.J. Altstetter, Hydrogen-enhanced localization of plasticity in an austenitic stainless steel, Metall. Mater. Trans. A, 1995, vol. 26, no. 11, pp. 2859-2871.
15.    M. Koyama, E. Akiyama, T. Sawaguchi, K. Ogawa, I.V. Kireeva, Y.I. Chumlyakov, K. Tsuzaki, Hydrogen assisted quasi-cleavage fracture in a single crystalline type 316 austenitic stainless steel, Corros. Sci., 2013, vol. 75, pp. 345-353.
16.    Y. Mine, Z. Horita, Y. Murakami, Effect of hydrogen on martensite formation in austenitic stainless steels in high-pressure torsion, Acta Mater., 2009, vol. 57, no. 10, pp. 2993-3002.
17.    Y. Mine, C. Narazaki, K. Murakami, S. Matsuoka, Y. Murakami, Hydrogen transport in solution-treated and pre-strained austenitic stainless steels and its role in hydrogen-enhanced fatigue crack growth, Int. J. Hydr. Energy, 2009, vol. 34, no. 2, pp. 1097-1107.
18.    A.F. Padilha, R.L. Plaut, P.R. Rios, Annealing of cold-worked austenitic stainless steels. ISIJ Int., 2003, vol. 43, no. 2, pp. 135-143.
19.    V. Shrinivas, S.K. Varma, L.E. Murr, Deformation-induced martensitic characteristics in 304 and 316 stainless steels during room-temperature rolling, Metall. Mater. Trans. A, 1995, vol. 26, no. 3, pp. 661-671.
20.    E. Astafurova, A. Fortuna, E. Melnikov, S. Astafurov, The effect of strain rate on hydrogen-assisted deformation behavior and microstructure in AISI 316L austenitic stainless steel, Materials, 2023, vol. 16, no. 8, art. no. 2983.
21.    Y. Yagodzinskyy, O. Todoshchenko, S. Papula, H. Hänninen, Hydrogen solubility and diffusion in austenitic stainless steels studied with thermal desorption spectroscopy, Steel Res.Int., 2011, vol. 82, no.1, pp. 20-25.
22.    D.B. Williams, C.B. Carter, Transmission Electron Microscopy. Textbook for Materials Science, Springer, New York, USA, 2009.
23.    I. Shakhova, V. Dudko, A. Belyakov, K. Tsuzaki, R. Kaibyshev, Effect of large strain cold rolling and subsequent annealing on microstructure and mechanical properties of an austenitic stainless steel, Mater. Sci. Eng. A, 2012, vol. 545, pp. 176-186.
24.    C. Donadille, R. Valle, P. Dervin, R. Penelle, Development of texture and microstructure during cold-rolling and annealing of f.c.c. alloys: example of an austenitic stainless steel, Acta Metall., 1989, vol. 37, no. 6, pp. 1547-1571.
25.    O.V. Rybalchenko, D.V. Prosvirnin, A.A. Tokar, V.P. Levin, M.R. Tyutin, G.I. Raab, L.R. Botvina, S.V. Dobatkin, Effect of ECAP on structural, mechanical and functional characteristics of the austenitic Cr-Ni-Ti steels, J. Phys.: Conf. Ser., 2018, vol. 1134, art. no. 012049.
26.    S.V. Dobatkin, O.V. Rybalchenko, N.A. Enikeev, A.A. Tokar, M.M. Abramova, Formation of fully austenitic ultrafine-grained high strength state in metastable Cr-Ni-Ti stainless steel by severe plastic deformation, Mater. Lett., 2016, vol. 166, pp. 276-279.
27.    A.K. De, J.G. Speer, D.K. Matlock, D.C. Murdock, M.C. Mataya, R.J.Comstock, Deformation-induced phase transformation and strain hardening in type 304 austenitic stainless steel, Metal. Mater. Trans. A, 2006, vol. 37, no. 6, pp. 1875-1886.
28.    E.I. Galindo-Nava, P.E.J. Rivera-Díaz-del-Castillo, Understanding martensite and twin formation in austenitic steels: A model describing TRIP and TWIP effects, Acta Mater., 2017, vol. 128, pp. 120-134.
29.    C. Zhang, H. Zhi, S. Antonov, L. Chen, Y. Su, Hydrogen-enhanced densified twinning (HEDT) in a twinning-induced plasticity (TWIP) steel, Scr. Mater., 2021, vol. 190, pp. 108-112.
30.    M. Koyama, N. Terao, K. Tsuzaki, Revisiting the effects of hydrogen on deformation-induced γ-ε martensitic transformation, Mater. Lett., 2019, vol. 249, pp. 197-200.
31.    J.S. Aristeidakis, G.N. Haidemenopoulos, Constitutive and transformation kinetics modeling of ε-, α′-martensite and mechanical twinning in steels containing austenite. Acta Mater., 2022, vol. 228, art. no. 117757.
32.    E.G. Astafurova, M.S. Tukeeva, G.G. Maier, E.V. Melnikov, H.J. Maier, Microstructure and mechanical response of single-crystalline high-manganese austenitic steels under high-pressure torsion: The effect of stacking-fault energy, Mater. Sci. Eng. A, 2014, vol. 604, pp. 166-175.
33.    I.V. Kireeva, Y.I. Chumlyakov, Effect of nitrogen and stacking-fault energy on twinning in [11] single crystals of austenitic stainless steels, Phys. Metals Metallogr., 2009, vol. 108, no. 3, pp. 298-309.
34.    I.V. Kireeva, Y.I. Chumlyakov, Orientation dependence of the γ-ɛ martensitic transformation in single crystals of austenitic stainless steels with low stacking fault energy, Phys. Metals Metallogr., 2006, vol. 101, no. 2, pp. 186-203.
35.    X.-S. Yang, S. Sun, T.-Y. Zhang, The mechanism of bcc α′ nucleation in single hcp ε laths in the fcc γ → hcp ε → bcc α′ martensitic phase transformation, Acta Mater., 2015, vol. 95, pp. 264-273.
36.    M.J. Sohrabi, M. Naghizadeh, H. Mirzadeh, Deformation-induced martensite in austenitic stainless steels: A review, Archiv. Civ. Mech. Eng., 2020, vol. 20, no. 4, art. no. 124.
37.    V.A. Polyanskiy, A.K. Belyaev, E.L. Alekseeva, A.M. Polyanskiy, D.A. Tretyakov, Yu.A. Yakovlev, Phenomenon of skin effect in metals due to hydrogen absorption, Continuum Mech. Thermodyn., 2019, vol. 31, no. 6, pp. 1961-1975.
38.    E. Owczarek, T. Zakroczymski, Hydrogen transport in a duplex stainless steel, Acta Mater., 2000, vol. 48, no. 12, pp. 3059-3070.
39.    V. Olden, C. Thaulow, R. Johnsen, Modelling of hydrogen diffusion and hydrogen induced cracking in supermartensitic and duplex stainless steels, Mater. Des., 2008, vol. 29, no. 10, pp. 1934-1948.
40.    H. Zhan, Y. Li, W. Liang, L. Zheng, Observation of diffusion channel and hydrogen trap in 304 austenitic stainless steel, Mater. Lett., 2021, vol. 290, art. no. 129453.
41.    I.M. Robertson, The effect of hydrogen on dislocation dynamics, Eng. Fra. Mech., 2001, vol. 68, no. 6, pp. 671-692.

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Поступила в редакцию: 20 Сентября 2024

Принята: 25 Сентября 2024

Доступна онлайн: 30 Сентября 2024

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